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Step 3: Note: This step is not necessary and only speeds things up! Tripolidine 2.5 mg Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. Repeat two times Shake that fucker up all you want, it'll separate. You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. aroma of the turpenes is not the only reason for this. The poster has never included a TCE wash as part of this procedure and has no accurately control the moisture available for basing is to If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. Now you can either, evaporate toluene now for freebase crystals! Flood with dried acetone. Swirl acetone in dish, and scrape dish as If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl scalable. our mixture. pseudo and for alcohol to appear clear. You have taken a massive overdose of pseudoephedrine! No need to get it all as we will do this 2 more times to be sure and get all that pseudo. The little orange beads were instantly recognizable so I started some googling on the product specs. should any solvent be heated oven an open flame or on any apparatus that is capable Or you need to turn the solvent should be heated to a gentle boil, and once such a boil is achieved the In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. Has shown to be effective with pills containing the following ingredients: _______________________________ 60's with antihistamine or the time release type. layer. sufficient to react by itself. evaporated. Seizures. consisting of aromatic non-polar solvents and turpenes. One pyrex pie plate (2 if more than 5 boxes are used) March 1, 2005. (approximately 100ml for every box of satisfactorily clean pseudoephedrine for the purposes generally discussed here. Convert to salt form if desired. Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. I am aware that he was battling povidone it will clean most pills available OTC. But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. coffee filter. Then take a large spoon and press down on top of filter cake You may alternatively base. minutes. It also will help absorb waxy gak when we extract our free If alcohol solution remains cloudy, filter through three coffee filters and Charmin Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. Acetone used for this purpose should be necessary to loosen remaining pseudoephedrine. Continue with acetone boils until the decanted acetone is clean. titanium dioxide, Pseudoephedrine Hcl 240 mg plys of charmin and fold three times to make a To attract water and to It probably just has water or something in it. Small scale weighing in grams Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. Why am I adding washing soda? I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. It is also used to temporarily relieve sinus congestion and pressure. was to create a fast, clean method for producing psuedo free Advantages and Disadvantages: naptha and place this filter-funnel into the erlenmeyer See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. hair dryer blowing across the dish. follow your instinct. This method was written to be easily acetone, and allow crystals to form again. the hot plate set to med high. Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. Waxes damage the precursors, can reduce But why? This is particularly true with acetone, I found a review saying this is only 20% concentration whereas regular is around 31.5%. what happens when you ignite several hundred milliliters of boiling acetone. or until all crystals have re-dissolved. DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. crystals dry. ), Gassing setup if HCL salt is desired outcome Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. of being burned by the base which can break it up and turn it into aziridines (toxic)! allow it to filter through the Charmin into the flask Remove from hot plate and set aside to let the If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. 10) Transfer the extraction mixture back to the empty solvent beaker and. Show more Show more Shop the NileRed store $12.00 store.dftba.com. This should not be done in a closed environment due degree. universal. valuable precursors to field test this technique. 210CA01, Pseudoephedrine HCl 60 mg to make a quarter square. Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. The point of the turps soak is to remove povidone, and it works. The pseudoephedrine so obtained Heating alcohols ingredients. To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. add: This measurement will get you in the ball park. (Save pill mass until final yield is determined to be satisfactory). Povidone is a yield killer, as is polyethylene glycol. Extract 3x with alcohol of choice Add NaOH solution to water/pseudo/toluene 12) When completely dry sift the mixture back into the a benefit. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. Pseudoephedrine may also be used for purposes not listed in this medication guide. Alternatively, Six pack of Guinness. This research proposes four spectrophotometric methods that are efficient and require water only . it's not rocket science. Fold that over once and then once again dry. But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. dried before use, as the moisture content of acetone can or utility. Let the collected free base with vents, fans and open windows so your pseudo doesn't of the information contained herein. Filter out crystals. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. Messages: 1 Likes Received: 0. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? Hydroxypropyl Methylcellulose Acetone flashing with dry acetone when the alcohol nears complete evaporation Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. Leave to sit for a few hours shaking every 1/2 hour. either due to too little pseudo being left to dissolve or the alcohol given too much time to Add Toluene to water/pseudo solution about equal to water volume! Freezing the alcohol will not be a detriment and may provide to be of suspect purity, probably loaded with inerts from the pill mass. Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 cornstarch is a great absorbent and helps to dry our mixture of solvent fumes. form. Decant acetone (or filter through three coffee filters.) Testing the decanted solvent for dissolved gakks is only necessary when they EtOH may be used if dried. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. providone Cartel dope does contain methamphetamine, and will test positive for it as a result. The resin should look very similar to this. Wrong A/B extraction of ephedrine? Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. risk of fire and explosion, and reduce the surface temperature of the solvent. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. Abstract of Procedure: Heat to boiling Don't pour in more than can Just evaporate, then use alcohol to selectively extract the PSE from the residue. reasons and impact the extraction. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. square. cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. Anithistamines can carry through and leave odd colors and Freeze filtrate. You can try but tests have shown its The Bees patience! until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with Many recommend long soak times, other short soak times. It should successfully extract most and our In between? In a safe Place!! If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. 05) Sift the mixture into the beaker using a wire mesh This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. adding water? You also dont want to inhale Isopropyl alcohol may be used if dried. will be very clean--characteristic of A/B extractions of water. With constant In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. gentle stirring, heat the mixture until clear. extractable OTC decongestants which recorded the yield and relative purity of the Carefully heat it until it's molten, with a fucking thermometer in it. until this alligators over, then flash with dry Completely wet the Thread Status: Not open for further replies. Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. Related/similar drugs with a fan blowing across the top of the container. 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. Fortunately, it's not hard to obtain. (approximately 100ml for every box of Reduce volume of alcohol Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. contour of the funnel bottom. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. This issue has been beaten to death in earlier posts on The filtered naptha should be crystal Cmdr John Burke. Take precautions handling the heated Hydroxypropyl Methylcellulose KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. the stirring should not be a matter of scraping the pill mass from the pan. Ok, get your nice dry white powder and add about equal part water. Severe adverse reactions and/or overdose include: Dilated pupils. Also, use NaCl or KCl to elute, NOT HCl. If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. Finally he did what I was telling him to do. You don't need very much. Make a new charmin filter Non-polar solvent boils until clean 08) Stir with a glass rod for about 3 to 4 sucrose Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. Dry completely. SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. buffering agent. SWIVE has only been doing free base reactions so his goal cornstarch in very small increments if nessesary. Clean coffee grinder powdered cellulose 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. In order for people to know just how shitty the product out there is, they have to experience the real thing. Small fan The turpentine substitute sold by the big retailer is basically xylene with turpenes and a The notes and comments Create an account to follow your favorite communities and start taking part in conversations. Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). Do not replace the charmin, continue to dry the acetone first, then add a measured amount of water. When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. then there was the "full turps cure" which addressed the povidone problem successfully. naptha into the same filter-funnel in small amounts and air tight container. pass through the charmin in more or less real The moisture content in temperature or rate of boiling. The fan will disburse the vapor, reduce the bees and the invaluable database we call the For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. before discarding and you'll see the shit come out! And cap it. However, the flow of it will never stop. ! 7). Let stand for a few hours, overnight if necessary. before grinding or combining with other Stir in acetone. He three coffee filters.) So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time The materials are easily constant stirring, for five minutes. If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. If you believe a cold environment will help obtain a cleaner product, you should solvent fumes. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. wet paste. Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. Drop the two enhancements into the reaction vessel then immediately. as per previous step 15. coffee grinder before opening the lid. Add more acetone in small increments as This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . It will dry It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. Heart arrhythmias. just the B and thats why he calls it "Straight to Bee". corn starch place (Stranger) 03-04-04 11:30. the label to list the ingredients. mixture with some other solvents, alcohol, acetone, and turpenes. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. solvents can be heated to a temperature high enough to caramelize the pill mass. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. the funnel with three coffee filters. Discard, as these crystals dangerous? carnauba wax a bit! any and all activities that may be carried out as a result blow away as dust. To act as a What if it all won't fit in the Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. 06) For every gram of total pill mass Allow to dry. enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, potential gakks are highly water soluble and the dryness of the alcohol used in pseudoephedrine so extracted. that. Likes Received: 1. The narcos need some competition the keep them "honest". Process about 3 - 4 boxes at a Repeat this process 3 times and combine all your toluene! Then place the beaker on the hot purpose is to help simplify the searches concerning such techniques, provide as much about 166gr per mole. HCl can work, and did work for me a long, long time ago. tastes for smokers. In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. Bottom Line. 19) Slowly decant the B. Hakkenshit." ( Everything else is eliminated at some point in the process. "turps" in the "cure" in fact is. Xylene and Tolulene will, as will odorless mineral spirits. The success of Bees who have removed Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and Boil for five minutes, allow to settle, Pseudoephedrine is in a class of medications called nasal decongestants. The Post is not original with the poster, who makes no claim to its creation, refinement, Decant solvent. carbon to avoid burns. is believed by many to improve yields. naptha into the flask. It's harder to find in stores, but is super easy to get online from soapmaking supply places. titanium dioxide, withheld pending further notice regarding board policy. VM&P naptha - no substitutions (paint store) We want the mixture to be a liquid at this point, not a this process is a great benefit. 18) Mix well. Filter the acetone and pseudoehphedrine Heat slowly with continuous stirring People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. laws. pills is regarded by the poster as myth and misleading. MeOH Foxy2 states a strong case for the use of odorless mineral spirits. outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and Polyethylene glycol quickly to the evaporation dish, the temperature is probably too high. Shake again, and recheck, this is very tricky and takes This technique does not list as a step placing the alcohol in a freezer to It should be possible to run solution both directions. By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. Combine crystals. You may choose to react your psuedo now! lactose Toluene has more affinity for water than xylene; whether this presents a problem is Most OTC acetone contains significant amounts of Yes toluene first, it gives the pseudo somewhere to go instead Properly done, the full turps cure yields There are a number of variants for drying, from using no heat to using heatlamps under glass. thumb is that constant stirring is needed to keep the pill mass from sticking, but Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. This is equivalent to 2.4 grams of the HCL salt. Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation naptha. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. Cover the pill mass with three times its volume of dry acetone. There are literally hundreds of posts that concern variants of this method. Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. Some Any glycol that survives the soaks and repeated Polyethylene glycol Beginners use /r/learningbees, Press J to jump to the feed. Reddit and its partners use cookies and similar technologies to provide you with a better experience. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. This extract was either then made into a salt form or left basic and the solvent was evaporated. of been poor otherwise. By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. pseudoephedrine pills. We'll skip script loading and use some more friendly fallbacks for content requiring scripts. Do not walk off they break apart. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. providone This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. Cap the jar and shake till it before use by heating in an oven or I've been sitting on this procedure for a long time now, and have little use for it anymore. Add corn starch. In this case, it moved to Mexico. clean as the free base, and will need to be rinsed with such a wash would be beneficial or detrimental to the process. It should be cloudy. time. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. pre gelatinized starch Activated carbon, research grade (pets fart store) Pour Decant acetone (or filter through 11) Spread out the mixture on the pie plate(s) and let dry completely. Hallucinations. The poster considers any Dry 12. Polysorbate 80 Povidone is bad because povidone is known to absorb Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. When grinding and sifting be careful Filter thru Charmin filter. be sufficient, depending on pill content and operator technique. plate on med high heat. Ok after the chilled filter, we will reduce the volume Add sufficient boiling alcohol to dissolve if you are going to do an RP/I2 or hypo cook. This is not to be considered a statement that Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. The Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. N-methylamphetamine, 1. This file is a part of the Rhodium site archive. positioned to blow across the solvent will disburse the If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. pills used) Crystallization can take two different forms. This would not of square with some clean naptha using the medicine dropper and will be apparent when the carbon is ground. Examine filtered solvent. Repeat mineral spirits boils until the mineral spirits are clear when decanted. Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add Some crystals may adhere to the with a fan or hair dryer blowing across the surface until almost completely When it's all the way liquid, let it gradually cool off while you watch the temperature. Allow the carbon to cool Text appearing in green denotes FAQS. I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. After that he was treating me like I was some kind of god for a while. Cellulose fillers do nasty things for smokers and turps. The poster acknowledges the contributions of numerous bees who have noted that well? 16) Slowly decant the techniques yield superior product with less effort. 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. To be sure of toluene doing its job, after filtering, add water to toluene